| Publication Type |
Journal Article |
| School or College |
College of Engineering |
| Department |
Materials Science & Engineering |
| Creator |
Ostafin, Agnes |
| Other Author |
Dai, Qing; Menzies, David; Wang, Qiang; Brown, Seth N.; Miesel, Dan; Maginn, Edward J. |
| Title |
Monitoring the synthesis and composition analysis of microsilica encapsulated acetylacetonatocarbonyl triphenylphosphinerhodium catalyst by inductively coupled plasma (ICP) techniques |
| Date |
2006 |
| Description |
Abstract-A novel technique to monitor the synthesis process of encapsulated acetylacetonatocarbonyl triphenylphosphinerhodium within a microsilica nanoshell has been studied using inductively coupled plasma (ICP) techniques. Nanospheres sized around 50-100 nm were obtained and ICP was used to quantify the exact composition of rhodium, phosphorous, and silicon with differing digestion solvents. In addition, ICP was used to detect rhodium and phosphorous in the nano core-shell catalysts as a quality control procedure. Index Terms-Encapsulation, inductively coupled plasma (ICP), nanotechnology, Rh catalyst, silica nanoshell. |
| Type |
Text |
| Publisher |
Institute of Electrical and Electronics Engineers (IEEE) |
| Volume |
5 |
| Issue |
6 |
| First Page |
677 |
| Last Page |
682 |
| Language |
eng |
| Bibliographic Citation |
Dai, Q., Menzies, D. B., Wang, Q., Ostafin, A. E., Brown, S. N., Miesel, D., & Maginn, E. J. (2006). Monitoring the synthesis and composition analysis of microsilica encapsulated acetylacetonatocarbonyl triphenylphosphinerhodium catalyst by inductively coupled plasma (ICP) techniques. IEEE Transactions on Nanotechnology, 5(6), 677-82. November. |
| Rights Management |
(c) 2006 IEEE. Personal use of this material is permitted. However, permission to reprint/republish this material for advertising or promotional purposes or for creating new collective works for resale or redistribution to servers or lists, or to reuse any copyrighted component of this work in other works must be obtained from the IEEE. |
| Format Medium |
application/pdf |
| Format Extent |
2,383,933 bytes |
| Identifier |
ir-main,15421 |
| ARK |
ark:/87278/s6gj02c4 |
| Setname |
ir_uspace |
| ID |
705019 |
| Reference URL |
https://collections.lib.utah.edu/ark:/87278/s6gj02c4 |
